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6.3 The preset boxes: Apertures and Mass

Mass & Apertures
Calib Tools Mass
Direct Calib
Shift Mass Center Mass CallCalib
Sample HV offset (V): 0
Calib
Direct Calib adds the line (M, B) to the current [M, B] table.
Shift Mass shifts all the [M, B] table according to the ratio (M1/M2) by modifying the Mass in the [B, k(B)] table (Refer to the secondary ion optics guide for information about the [B, k(B)] table).
Call Calib opens the Mass calibration routine.
Mass & Apertures
Calib Tools Mass
Set M Aperture init
28Si Sample offset
27.93 Clear Energy Slit X offset
Sample HV offset (V): 0
Tools
Aperture init opens the Aperture Init box (See below).
Sample offset opens the Sample HV offset box (See below).
Clear Energy Slit X offset resets the Energy Slit X to zero for all energy slit presets.
Mass & Apertures
Calib Tools Mass
Set Mass Mass Centering
28Si Clear List of mass
27.9769 Apply
Mass
Mass Centering opens the Scan All dialog box. The magnetic field is scanned around the initial value.
Clear List of mass removes recently called masses on a scroll down list of Set Mass box.
Mass & Apertures
Calib Tools Mass
Set Mass
28Si Center Mass 27.9769 Apply
Sample HV offset (V): 0
Set Mass edits the required mass, validated by the computer kbd Enter or by clicking Apply.
Center Mass button is the same function as Mass Centering.
Apply loads the edited mass to the instrument.
▲▼ increments the mass of +/- 1 amu.

These presets directly control the instrument. Before starting an analysis, it is advisable to select the presets corresponding to the status of the instrument, since this information is stored in the data files.

Mass & Apertures and Energy Presets windows
  • D0 allows to assign the aperture preset pad to select the first primary aperture.
  • D4 allows to assign the aperture preset pad to select the second primary aperture.
  • CA/FA/Ent/Ener/Exit allows to assign the aperture preset pad to the selected aperture:
    • CA stands for Contrast Aperture.
    • FA stands for Field Aperture.
    • Ent stands for Entrance slit.
    • Ener stands for Energy slit.
    • Exit stands for Exit slit.

For example, it is explained that the Exit Slit and the Entrance slit presets cannot be changed, that Exit Slit is expressed as a MR (Mass resolution) while Entrance Slit is expressed in µm.

For any selection of D0/D4/CA/FA apertures and Ent/Ener/Exit slits, Calib does not open the Calib box but assigns the keyboard thumbwheels to the selected aperture axis.

Valid modifies the preset content, if the Valid is enabled, that is the case for D0, D4, CA, FA and Ener.

By clicking the M. Reso. button opens the Mass Resolution preset box on the right-hand side.

Center button is available at the bottom of the preset panel in case of Contrast Aperture (CA) and Entrance slit (Ent). Center launches automatic centering procedure by Scan All program.

Adjust button is available at the bottom of the preset panel only for Energy slit (Ener). Adjust launches automatic adjust procedure by Scan All program.

Remark 1: The 3 slits labels cannot be entered since they are determined automatically from the actual aperture position. The Exit Slit label is in MR, the Entrance slit label is in µm and the Energy Slit in eV. If the labels are observed to be wrong, the expert operator must check the slit offset (in the Interface window, select the utility menu “Aperture and Stage”, and there it is possible to select Entrance width offset / Exit width offset / Energy width offset / Energy slit position). These functions must be activated after the operator has set respectively the Entrance width, the Exit width and the Energy width to zero or the low energy edge to axis.

Remark 2: After the motorization chassis is switched off, the aperture positions considered by the instrument and displayed in the user’s interfaces are no more correct. It is necessary to activate Init procedures.